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Beilstein J. Org. Chem. 2019, 15, 2059–2068, doi:10.3762/bjoc.15.203
Graphical Abstract
Figure 1: Quinoxaline derivatives 1–3.
Scheme 1: Synthesis of THTTA (3).
Scheme 2: Protonation, alkylation and acylation of 3.
Figure 2: The ORTEP view of 3. Torsion angles within the benzene ring are given in red.
Figure 3: The ORTEP view of 6a. Torsion angles within the benzene ring are given in red.
Figure 4: The ORTEP view of 7a (the iodine counter anion has been omitted for clarity). Torsion angles within...
Scheme 3: Charge transfer and delocalization within 3 and its diprotonated (6a) and monomethylated (7a) deriv...
Figure 5: Normalized absorption spectra of 3 in: toluene (black), acetone (blue), ethanol (green), water (red...
Figure 6: Protonation of 3 in ethanol. Two isosbestic points (IBP) are indicated by arrows.
Figure 7: Absorption spectra of 7a (blue) and 8 (red) in ethanol.
Figure 8: Absorption spectra of 10a (black), 10b (red). Solid curves: in toluene, dashed curves: in acetone.
Figure 9: View of the supramolecular array generated by 3 in the solid state. Color coding: nitrogen, blue; c...
Figure 10: View of the supramolecular array generated by 6a in the solid state. Color coding: nitrogen, blue; ...
Figure 11: View of the supramolecular array generated by 7a in the solid state. Color coding: nitrogen, blue; ...